The VTA VK100-10 vacuum distillation system is an advanced device
designed for effective separation of substances under reduced pressure
conditions. It is particularly useful in processes requiring gentle
treatment of materials sensitive to high temperatures.
Key features of the VTA VK100-10 system:
• Efficiency: The ability to process large quantities of material,
making it suitable for industrial applications.
• Precise parameter control: The advanced control system allows for
precise monitoring and regulation of temperature and pressure,
ensuring optimal conditions for the distillation process.
• Safety: Equipped with advanced security systems, it protects
against potential hazards associated with working in a vacuum.
• Versatility: The ability to adjust operating parameters to
different types of materials, making the system universal in
industrial applications.
The VTA VK100-10 system is the ideal solution for companies looking
for an efficient and safe way to carry out vacuum distillation on an
industrial scale.
The VTA VK100-10 vacuum distillation kit includes the following
components:
1. Distillation column – the main element for carrying out the
distillation process.
2. Vacuum pump (2x) – to maintain low pressure in the system.
3. Evaporator – to heat the liquid and evaporate it.
4. Condenser – to condense the steam into a liquid.
5. Two distillate collection lines – to collect separated
fractions.
6. Control system – to monitor and regulate temperature, pressure
and flow.
7. Valves and fittings – to control the flow of substances in the
system.
Technical data of the distillation unit:
Type of evaporator VK 100-10
Maximum distillation temperature 300 °C
Minimal achievable operating pressure (depending on product) < 10-3
mbar with rotary vane and oil diffusion vacuum pump,
Throughput 1 – 10 l/h (depending on product)
Evaporation surface 0.10 m²
Surface of internal condenser 0.15 m²
Other general data:
• Receivers are fabricated in Borosilicate-Glass
• Evaporator, feed tank, cold traps, wiper basket and rotary
transmission are
fabricated in stainless steel
• Gaskets are fabricated in FKM (Viton)
• All glass connections will be manufactured with standard grindings
or ball grindings.
• The unit will be equipped with a power distribution system.
Customer supply will be
400 volts / 50 Hz / 3-phases / loadable neutral line / physical
earth.
• All electrical consumers will be CE marked (European standard).
Applied standards: EN (European Standard) and DIN (German Industrial
Standard) American standards have not been considered.
• None of the equipment is in explosion proof design
Detailed specification:
Pos. 1. Feed
Feed tank in stainless steel in jacketed design with flanged lid with
spare nozzles: 10 Liter
Gear pump in jacketed design (design temperature 300°C), the speed of
the pump is adjustable by frequency inverter. Frequency inverter is
located at plant skid: Max. 14.0 l/h
Feed line to evaporator in jacketed design
Drain valve (not jacketed)
Overflow valve in heatable design
Pos. 2. Short-Path Evaporator VK 100-10
Evaporator surface : 0.10 m²
Internal condenser (bundle) : 0.15 m²
Wiper basket with vacuum rotary transmission : SKR block rotor
Gasket of transmission : Lip sealing
Material of fabrication : 1.4571 (316 Ti) or 1.4404 (316L)
Number of wiper strands : 3
Wiper basket drive continuously variable: Yes
Digital display of wiper speed at motor drive : Yes
Evaporator temperature : Max. 300 °C
Operating pressure (depending on product) : 0.001 mbar
SKR wiper blocks : Graphite
Product nozzles : Tri-Clamp 2”
Vacuum nozzle : KF 50
Nozzle for heating medium : DN 15 „special
Residue nozzle in jacketed design : Yes
Distillate nozzle in heatable design : Yes
Pos. 3. Distillate and residue discharge (each)
Jacketed sight glass
Gear pump in jacketed design: Max. 14.0 l/h (design temperature
300°C), the speed of the pump is adjustable by frequency inverter.
Frequency inverter is located at plant skid
Discharge siphon after the gear pump in jacketed design (used as
pressure lock against the atmosphere).
Pos. 4. Vacuum System
Flanged cold trap for liquid chilling media with receiver in glass (1
liter)
Flanged cold trap for liquid N2 or dry ice with receiver in glass (1
liter)
Oil diffusion vacuum pump for achieving stable vacuum conditions at
low pressures: 40 l/s
Two stage rotary vane pump with exhaust filter: 16.0 m³/h
Vacuum pump equipped with vacuum pump oil dosing valve for pressure
adjustment
and for venting
1 vacuum measuring device with one gauge.
Digital display.
Measuring range 0.0005 mbar – 1,300 mbar
All necessary connection pipes or hoses to the vacuum system
Pos. 5. Heating and Cooling
Heating unit
1 independent heating unit for - evaporator jacket
Circulation thermostat with digital temperature adjustment and numeric
display, including circulation pump
Temperature range: 300 C. st
Power: 3 kW
Medium (not in scope of supply): thermal oil
The system will be equipped with all necessary connecting hoses
(thermo insulated tubes made of stainless steel) to connected to the
unit.
Heating unit
1 independent heating unit for - Residue line
Circulation thermostat with digital temperature adjustment and numeric
display, including circulation pump
Temperature range: 200 st. C
Power: 2 F5760769 kW
Medium (not in scope of supply): thermal oil
The system will be equipped with all necessary connecting hoses
(thermo insulated tubes made of stainless steel) to connected to the
unit. All necessary jumpers in the heated lines are included as
well.
Heating unit
1 independent heating unit for - feed line
Circulation thermostat with digital temperature adjustment and numeric
display, including circulation pump
Temperature range: 200 st. C
Power: 2 kW
Medium (not in scope of supply): thermal oil
The system will be equipped with all necessary connecting hoses
(thermo insulated tubes made of stainless steel) to connected to the
unit. All necessary jumpers in the heated lines are included as
well.
Cooling unit (Placed next to skid)
1 independent cooling unit for - internal condenser and distillate
discharge line
Circulation thermostat with digital temperature adjustment and numeric
display, including circulation pump connected to cooling or tap
water
Temperature range (rating): -10 … 100 °C 2 Heating Power: 2.2 kW
Cooling power 15°C: 2,2 kW
Medium (not in scope of supply): Depending on temperature
The system will be equipped with all necessary connecting hoses
(thermo insulated tubes made of stainless steel) to connected to the
unit. All necessary jumpers in the heated lines are included as
well.
Chilling unit
1 independent cooling unit for - cold trap
Circulation thermostat with digital temperature adjustment and numeric
display, including circulation pump connected to cooling or tap
water
Temperature range (rating): -40 … 200 °C
Heating Power: 2 kW
Cooling power 0°C: 0.38 kW
Cooling power - 20°C: 0.25 kW
Medium (not in scope of supply): Depending on temperature
The system is equipped with all necessary connecting hoses (thermo
insulated tubes made of stainless steel) to connected to the unit. All
necessary jumpers in the heated lines are included as well.
Pos. 6. Rack/Frame, connectors
Frame made of stainless steel pipes (DN 32) with connection clamps for
variable use. The is equipped with 4 wheels and is moveable.
Collecting tray for leaking liquid is included.
Pos. 7. Power supply to power distribution system (by customer)
Voltage: 400 V
Frequency: 50 Hz
No of phases:3
Power distribution system included: Yes
Frequency inverters located at plant skid: Yes